N-甲基-N-羟乙基苯胺合成路线 (共 41 条)
反应条件
72 h; UV-irradiation;
参考文献
Kim, Sung Sik; Mah, Yoon Jung; Kim, Ae Rhan
Tetrahedron Letters, 2001 , vol. 42, # 47 p. 8315 - 8317
反应条件
1: 21 percent / 24 h / UV-irradiation 2: 3 percent / 72 h / UV-irradiation View Scheme
参考文献
Tetrahedron Letters, , vol. 42, # 47 p. 8315 - 8317
反应条件
T=90 - 100°C; im Rohr;
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>41, p. 937
参考文献
Nippon Kagaku Zasshi, , vol. 73, p. 331
Chem.Abstr., , p. 10492
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 145, p. 126
Bulletin de la Societe Chimique de France, , vol. <4> 3, p. 376
反应条件
1: benzene; phosphorus oxychloride 2: benzene; phosphorus oxychloride View Scheme
参考文献
Anker; Cook
Journal of the Chemical Society, 1944 , p. 489,491
反应条件
Beim Erwaermen des danach isolierten Reaktionsprodukts mit N-Methyl-formanilid und Phosphoroxychlorid in Benzol;
参考文献
Gen.Aniline Works.
Patent: US2141090 , 1936 ;
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s) T=180°C; 5 h;
参考文献
Tsuji, Yasushi; Huh, Keun-Tae; Watanabe, Yoshihisa
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 377 - 380
反应条件
potassium hydroxide in dimethyl sulfoxide T=20°C; 1.5 h;
参考文献
PHARMACIA CORPORATION
Patent: WO2003/99769 A1, 2003 ;
Location in patent: Page 47 ;
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate T=5°C; Vilsmaeir reaction; 0.5 h; 2: N-methyl-N-phenyl-N-(2-hydroxyethyl)amine T=20°C; 3 h;
参考文献
BECTON, DICKINSON AND COMPANY
Patent: WO2006/25887 A2, 2006 ;
Location in patent: Page/Page column 21; 44-45 ;