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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
乙酸苏合香酯
合成路线
（共 201 条）
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
phosphate buffer; lipase T=20°C;
参考文献
Laumen, Kurt; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1988 , p. 598 - 600
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
16197-93-6
+
16197-92-5
反应条件
lipase from Burkholderia cepacia (BCL) Enzymatic reaction; optical yield given as percent ee;
参考文献
Gao, Yan; Zhong, Runtao; Qin, Jianhua; Lin, Bingcheng
Chemistry Letters, 2009 , vol. 38, # 3 p. 262 - 263
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-04-0
反应条件
triethylamine in tert-butyl methyl ether T=50°C; 216 h; Inert atmosphereEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-05-1
反应条件
triethylamine in tert-butyl methyl ether T=50°C; 216 h; Inert atmosphereEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-06-2
反应条件
triethylamine in tert-butyl methyl ether T=50°C; 216 h; Inert atmosphereEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
365996-19-6
叔-丁基N-[(1R,2S)-2-氨基环戊基]氨基甲酸酯
+
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1205616-17-6
+
721395-15-9
(1R,2S)-1-(Boc-氨基)-2-氨基环戊烷
反应条件
Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 144 h; Inert atmosphereMolecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 12, # 16 p. 3602 - 3605
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 144 h; Inert atmosphereMolecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
365996-19-6
叔-丁基N-[(1R,2S)-2-氨基环戊基]氨基甲酸酯
+
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1205616-17-6
+
721395-15-9
(1R,2S)-1-(Boc-氨基)-2-氨基环戊烷
+
445479-01-6
(1S,2R)-2-氨基-1-(Boc-氨基)环戊烷
反应条件
triethylamine in tert-butyl methyl ether T=50°C; 216 h; Inert atmosphereEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
24424-99-5
二碳酸二叔丁酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-04-0
反应条件
1: benzyl (+/-)-cis-(2-aminocyclopentyl)carbamate; 1-acetyloxyethylbenzene With Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 144 h; Inert atmosphereMolecular sieveEnzymatic reaction; 2: di-tert-butyl dicarbonate in tert-butyl methyl ether 0.0833333 h; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
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