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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
乙酸苏合香酯
合成路线
（共 201 条）
24424-99-5
二碳酸二叔丁酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-05-1
反应条件
1: allyl (+/-)-cis-(2-aminocyclopentyl)carbamate; 1-acetyloxyethylbenzene With Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction; 2: di-tert-butyl dicarbonate in tert-butyl methyl ether 0.0833333 h; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
93-92-5
乙酸苏合香酯
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
16197-93-6
反应条件
cells of Marchantia polymorpha in phosphate buffer; ethanol pH=6.0; Title compound not separated from byproducts;
参考文献
Mantovani, Simone M.; De Oliveira, Luciana G.; Marsaioli, Anita J.
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 8 p. 1484 - 1489
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
24424-99-5
二碳酸二叔丁酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
1240201-06-2
反应条件
1: ethyl (+/-)-cis-(2-aminocyclopentyl)carbamate; 1-acetyloxyethylbenzene With Candida antarctica polyacrylamide-immobilized lipase B, Novozyme SP-435 in tert-butyl methyl ether T=28°C; 120 h; Inert atmosphereMolecular sieveEnzymatic reaction; 2: di-tert-butyl dicarbonate in tert-butyl methyl ether 0.0833333 h; optical yield given as percent eeenantioselective reaction;
参考文献
Quijada, F. Javier; Gotor, Vicente; Rebolledo, Francisca
Organic Letters, 2010 , vol. 12, # 16 p. 3602 - 3605
93-92-5
乙酸苏合香酯
+
123-82-0
异庚胺
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
16197-93-6
+
50789-57-6
反应条件
hydrogen; lipase B from Candida antarctica in toluene T=70°C; P=750.075 Torr; 48 h; Resolution of racemateEnzymatic reaction;
参考文献
Xia, Bo; Cheng, Guilin; Lin, Xianfu; Wu, Qi
European Journal of Organic Chemistry, 2014 , vol. 2014, # 14 p. 2917 - 2923
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
746564-13-6
反应条件
Candida antarctica lipase B in various solvent(s) T=28°C; 46 h; Further byproducts given;
参考文献
Gonzalez-Sabin, Javier; Gotor, Vicente; Rebolledo, Francisca
Tetrahedron Asymmetry, 2004 , vol. 15, # 3 p. 481 - 488
93-92-5
乙酸苏合香酯
→
反应条件
1445-91-6
(S)-(-)-1-苯基乙醇
+
1517-69-7
(R)-(+)-1-苯基乙醇
+
16197-93-6
+
16197-92-5
反应条件
sodium carbonate; Candida rugosa lipase in toluene T=20°C; 144 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Merabet-Khelassi, Mounia; Houiene, Zahia; Aribi-Zouioueche, Louisa; Riant, Olivier
Tetrahedron Asymmetry, 2012 , vol. 23, # 11-12 p. 828 - 833
42882-31-5
1-萘乙胺
+
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
+
72407-64-8
反应条件
molecular sieve; lipase B from Candida antarctica in 1,4-dioxane T=30°C; aminolysis; Enzymatic reaction;
参考文献
Garcia-Urdiales, Eduardo; Rebolledo, Francisca; Gotor, Vicente
Tetrahedron Asymmetry, 2000 , vol. 11, # 7 p. 1459 - 1463
2941-19-7
1-苯基丁胺
+
93-92-5
乙酸苏合香酯
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
molecular sieve; lipase B from Candida antarctica in 1,4-dioxane T=30°C; aminolysis; Enzymatic reaction;
参考文献
Garcia-Urdiales, Eduardo; Rebolledo, Francisca; Gotor, Vicente
Tetrahedron Asymmetry, 2000 , vol. 11, # 7 p. 1459 - 1463
93-92-5
乙酸苏合香酯
+
1886-26-6
去甲氟苯丙胺
→
反应条件
1517-69-7
(R)-(+)-1-苯基乙醇
反应条件
molecular sieve; lipase B from Candida antarctica in 1,4-dioxane T=30°C; aminolysis; Enzymatic reaction;
参考文献
Garcia-Urdiales, Eduardo; Rebolledo, Francisca; Gotor, Vicente
Tetrahedron Asymmetry, 2000 , vol. 11, # 7 p. 1459 - 1463
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