3,4-环氧-1-丁烯合成路线 （共 241 条）
反应条件
methyl(diphenyl)-phosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=25°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 38, # 17 p. 3081 - 3084
反应条件
T=130 - 140°C; P=760.051 Torr;
参考文献
Eastman Chemical Company
Patent: US6342614 B1, 2002 ;
Location in patent: Example 133 ;
反应条件
magnesium bromide in N,N-dimethyl-formamide T=130°C; 0.0416667 h;
参考文献
Petroleum Chemistry, , vol. 43, # 3 p. 167 - 169
反应条件
NHep4(1+)*I(1-); tributyl tin (1+); iodide in para-xylene T=109 - 117°C; 0.75 h;
参考文献
Eastman Chemical Company
Patent: US6342614 B1, 2002 ;
Location in patent: Example 327 ;
反应条件
potassium iodide; USY zeolite in various solvent(s) T=74.85°C; 24 h; var. nucleophiles and acids; var. solv. and time; Product distributionMechanism;
参考文献
Remans, Thomas J.; Van Oeffelen, Domien; Steijns, Matt; Martens, Johan A.; Jacobs, Pierre A.
Journal of Catalysis, 1998 , vol. 175, # 2 art. no. CA982018, p. 312 - 315
反应条件
O,O'-(R)-(1,1'-dinaphthyl-2,2'-diyl)-N,N'-di-(R,R)-1-phenylethylphosphoramidite; copper(II) bis(trifluoromethanesulfonate) in toluene T=-78 - 0°C; 5 h; Title compound not separated from byproducts;
参考文献
Pineschi, Mauro; Del Moro, Federica; Crotti, Paolo; Di Bussolo, Valeria; Macchia, Franco
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2099 - 2105
反应条件
in tetrahydrofuran T=20°C; 4 h; Product distribution; Further Variations:Reaction partnersSolventsreaction time;
参考文献
Equey, Olivier; Vrancken, Emmanuel; Alexakis, Alexandre
European Journal of Organic Chemistry, 2004 , # 10 p. 2151 - 2159
反应条件
triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 15 h; Ambient temperature;
参考文献
Larksarp, Chitchamai; Alper, Howard
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3709 - 3715
反应条件
triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 15 h; Ambient temperature;
参考文献
Larksarp, Chitchamai; Alper, Howard
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3709 - 3715
反应条件
aluminium trichloride in benzene 1 h; Ambient temperature;
参考文献
Baba, Akio; Seki, Kenji; Matsuda, Haruo
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2684 - 2688
