3,4-环氧-1-丁烯合成路线 (共 241 条)
反应条件
(R)-C4-TunePhos; sodium carbonate; [(ν3-allyl)PdCl]2 in tetrahydrofuran
T=25°C; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Trost, Barry M.; Horne, Daniel B.; Woltering, Michael J.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6607 - 6620
反应条件
methyl(diphenyl)-phosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
T=25°C; 1 h; var. of anhydrides, solvents, ligand of palladium; Product distribution;
参考文献
Bianchi, Daniele; Querci, Cecilia; Ricci, Marco; Santi, Roberto
Tetrahedron Letters, 1997 , vol. 38, # 17 p. 3081 - 3084
反应条件
O,O'-(R)-(1,1'-dinaphthyl-2,2'-diyl)-N,N'-di-(R,R)-1-phenylethylphosphoramidite; copper(II) bis(trifluoromethanesulfonate) in toluene
T=-78 - 0°C; 5 h; Title compound not separated from byproducts;
参考文献
Pineschi, Mauro; Del Moro, Federica; Crotti, Paolo; Di Bussolo, Valeria; Macchia, Franco
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2099 - 2105
反应条件
in tetrahydrofuran
T=20°C; 4 h; Product distribution; Further Variations:Reaction partnersSolventsreaction time;
参考文献
Equey, Olivier; Vrancken, Emmanuel; Alexakis, Alexandre
European Journal of Organic Chemistry, 2004 , # 10 p. 2151 - 2159
反应条件
(i) Et2O, (ii) CrO3*2Py, CH2Cl2; Multistep reaction;
参考文献
Anderson,R.J.
Journal of the American Chemical Society, 1970 , vol. 92, p. 4978 - 4979
反应条件
n-butyllithium in tetrahydrofuran; hexane
from -10 degC to room temp., then 2 h;
参考文献
Alcaraz, L.; Harnett, J. J.; Mioskowski, C.; Martel, J. P.; Gall, T. Le; et al.
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5449 - 5452
反应条件
tetraphenyl stibonium iodide in dichloromethane
T=45°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Fujiwara, Masahiro; Baba, Akio; Matsuda, Haruo
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1351 - 1357
反应条件
(i) nBuLi, hexane, THF, (ii) /BRN= 103170/, HMPT; Multistep reaction;
参考文献
Balme,G. et al.
Synthesis, 1979 , p. 508 - 510
参考文献
Ponomarew; Wodopjanowa
Chimija chim. Technol. (NDVS)Chem.Abstr., 1959 , p. 316
Chimija chim. Technol. (NDVS)Chem.Abstr., 1960 , p. 267
Show Details
Gibbs; Calcote
Journal of Chemical and Engineering Data, 1959 , vol. 4, p. 226,232,236
参考文献
Arseniyadis, Simeon; Gore, Jacques; Guenot, Pierre; Carrie, Robert
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1413 - 1418