3,4-环氧-1-丁烯合成路线 (共 241 条)
参考文献
Petrow
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 994
Chem.Abstr., 1943 , p. 1699
Show Details
Kadesch
Journal of the American Chemical Society, 1946 , vol. 68, p. 44
反应条件
Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Savu, Patricia M.; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 239 - 250
反应条件
Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Savu, Patricia M.; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 239 - 250
反应条件
in diethyl ether
T=-20°C;
参考文献
Cahiez,C. et al.
Synthesis, 1978 , p. 528 - 530
反应条件
potassium phosphate; PdBr2(CH3CN)2; triglyme (triethylene glycol dimethyl ether); potassium bromide
T=5°C; 4 h; Schlenk techniqueInert atmosphere; regioselective reaction;
参考文献
Hamasaki, Akiyuki; Maruta, Shuhei; Nakamura, Aki; Tokunaga, Makoto
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 11-12 p. 2129 - 2134
反应条件
tin(ll) chloride
1 h; Heating;
参考文献
Vyvyan, James R.; Meyer, Jennifer A.; Meyer, Korin D.
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 9144 - 9147
参考文献
Petrow; Al'bizkaja
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 1907; engl. Ausg. S. 2125
反应条件
[(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminato(2-)]cobalt(III) acetate; water in tetrahydrofuran
T=0 - 20°C; 72 h;
参考文献
Ready; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 11 p. 2687 - 2688
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C; 72 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315