3,4-环氧-1-丁烯合成路线 （共 241 条）
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
triethyl borane; S,S-DACHN; sodium hydrogencarbonate; 4-(N,N-dimethlyamino)pyridine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in dichloromethane
Hydrolysis;
参考文献
Trost, Barry M.; McEachern, Ernest J.
Journal of the American Chemical Society, 1999 , vol. 121, # 37 p. 8649 - 8650
反应条件
(AcO)[(S)-substituted salen]Co(III) in water
T=0°C; 12 h; Title compound not separated from byproducts.;
参考文献
Dey, Sangeeta; Powell, Douglas R.; Hu, Chunhua; Berkowitz, David B.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 37 p. 7010 - 7014
反应条件
[(S,S-N,N'-bis(3,5-bis(tert-butyl)salicylidene)-1,2-cyclohexanediamine)cobalt(II)]; acetic acid in water
18 h;
参考文献
Orac, Crina M.; Zhou, Shu; Means, John A.; Boehm, David; Bergmeier, Stephen C.; Hines, Jennifer V.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 19 p. 6786 - 6795
反应条件
sodium hydroxide; sodium tetrahydroborate; mercury(II) diacetate
other reducing agent; Product distribution;
参考文献
Brown, Herbert C.; Lynch, Gary J.
Journal of Organic Chemistry, 1981 , vol. 46, # 5 p. 930 - 939
反应条件
potassium carbonate in ethanol
8 h; Heating;
参考文献
Ahmed; Stratford; Jenkins
Arzneimittel-Forschung/Drug Research, 1985 , vol. 35, # 12 p. 1763 - 1768
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
T=35 - 40°C; Makosza procedure; 12 h; Product distribution; Further Variations:Reaction partners;
参考文献
Mannafov; Berdnikov; Samuilov
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 3 p. 339 - 344
反应条件
sodium in methanol
T=50°C;
参考文献
Silvestri, Maximilian A.; He, Chang; Khoram, Anita; Lepore, Salvatore D.
Tetrahedron Letters, 2006 , vol. 47, # 10 p. 1625 - 1626
参考文献
Van Zyl; van Tamelen
Journal of the American Chemical Society, 1950 , vol. 72, p. 1357
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=25°C;
参考文献
Trost, Barry M.; Cossy, Janine
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6881 - 6882
