3,4-环氧-1-丁烯合成路线 (共 241 条)
参考文献
Hamersma, J. A. M.; Nossin, P. M. M.; Speckamp, W. N.
Tetrahedron, 1985 , vol. 41, # 10 p. 1999 - 2006
参考文献
Kociolek, Martin G.; Hongfa, Chayanant
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1811 - 1813
反应条件
1: T=20°C; Allylboration; 168 h;
2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
T=20°C; Oxidation; 4 h; Further stages.;
参考文献
Zaidlewicz, Marek; Krzeminski, Marek P.
Organic Letters, 2000 , vol. 2, # 24 p. 3897 - 3899
反应条件
1: T=60°C; Allylboration; 24 h;
2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
T=20°C; Oxidation; 4 h; Further stages.;
参考文献
Zaidlewicz, Marek; Krzeminski, Marek P.
Organic Letters, 2000 , vol. 2, # 24 p. 3897 - 3899
反应条件
in diethyl ether
T=-78°C;
参考文献
Naruta, Yoshinori; Maruyama, Kazuhiro
Chemistry Letters, 1987 , p. 963 - 966
反应条件
di-n-butylboryl trifluoromethanesulfonate in dichloromethane
T=-78°C; 0.5 h;
参考文献
Naruta, Yoshinori; Maruyama, Kazuhiro
Chemistry Letters, 1987 , p. 963 - 966
反应条件
di-n-butylboryl trifluoromethanesulfonate in dichloromethane
T=-78°C; 0.5 h;
参考文献
Naruta, Yoshinori; Maruyama, Kazuhiro
Chemistry Letters, 1987 , p. 963 - 966
反应条件
n-butyllithium; cerium(III) chloride
1.) Et2O, RT, 1 h, 2.) Et2O, RT, 5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-ichi; Sakai, Shizuyoshi
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 12 p. 3308 - 3314
反应条件
chiral oligo-(salen)Co(OTs) complexes; lutidinium p-toluene sulfonate; water in dichloromethane; acetonitrile
T=20°C; 4 h;
参考文献
Ready; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 11 p. 2687 - 2688
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315