3,4-环氧-1-丁烯合成路线 （共 241 条）
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C; 72 h;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
(S,S)-[1,2-cyclohexanediamino-N,N'-bis(3,5-di-t-butylsalicylidene)]cobaltIII*OAc; water in tetrahydrofuran
T=0 - 20°C;
参考文献
Schaus, Scott E.; Brandes, Bridget D.; Larrow, Jay F.; Tokunaga, Makoto; Hansen, Karl B.; Gould, Alexandra E.; Furrow, Michael E.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2002 , vol. 124, # 7 p. 1307 - 1315
反应条件
water; (S,S)-(+)-Jacobsen salene complex in tetrahydrofuran
T=20°C; 84 h; Title compound not separated from byproducts.;
参考文献
Gierasch, Tiffany Malinky; Shi, Zhangjie; Verdine, Gregory L.
Organic Letters, 2003 , vol. 5, # 5 p. 621 - 624
反应条件
C64H74Cl2Co2N4O4; bis(triphenylphosphoranylidene)-ammonium acetate in toluene
T=0°C; 0.533333 h; Product distribution / selectivity;
参考文献
CORNELL RESEARCH FOUNDATION, INC.
Patent: WO2009/26261 A2, 2009 ;
Location in patent: Page/Page column 69; 74-75 ;
反应条件
(AcO)[(S)-substituted salen]Co(III) in water
T=0°C; 12 h; Title compound not separated from byproducts.;
参考文献
Dey, Sangeeta; Powell, Douglas R.; Hu, Chunhua; Berkowitz, David B.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 37 p. 7010 - 7014
反应条件
halohydrin dehalogenase (Agrobacterium radiobacter AD1,HheC); Tris-SO4 buffer in dimethyl sulfoxide
T=22°C; pH=7.5; 5 h; Title compound not separated from byproducts;
参考文献
Elenkov, Maja Majeric; Hauer, Bernhard; Janssen, Dick B.
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 4-5 p. 579 - 585
反应条件
(S,S)-(salen)Co(OAc) complex in water
optical yield given as percent de;
参考文献
Denmark, Scott E.; Nguyen, Son T.; Baiazitov, Ramil Y.
Heterocycles, 2008 , vol. 76, # 1 p. 143 - 154
参考文献
Petrow
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 994
Chem.Abstr., 1943 , p. 1699
反应条件
in diethyl ether
3.5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Yamada, Jun-ichi; Yumoto, Masatoshi; Yamamoto, Yoshinori
Tetrahedron Letters, 1989 , vol. 30, # 32 p. 4255 - 4258
参考文献
Bottini,A.T.; Dev,V.
Journal of Organic Chemistry, 1962 , vol. 27, p. 968 - 973
