3,4-环氧-1-丁烯合成路线 (共 241 条)
反应条件
tetrabutylammomium bromide; triphenylphosphine; zinc; NiCl2((PPh3)P)2 T=120°C; 1 h;
参考文献
Li, Fuwei; Xia, Chungu; Xu, Liwen; Sun, Wei; Chen, Gexin
Chemical Communications, 2003 , # 16 p. 2042 - 2043
反应条件
potassium hydroxide; carbon dioxide T=200°C;
参考文献
Jefferson Chem. Co.
Patent: US2773070 , 1952 ;
反应条件
in dichloromethane 1.) -78 deg C, 15 min, 2.) 25 deg C, 12 h;
参考文献
Lorincz, Tibor; Erden, Ihsan; Naeder, Reinhard; Meijere, Armin de
Synthetic Communications, 1986 , vol. 16, # 2 p. 123 - 130
反应条件
caesium carbonate in water T=25°C; 12 h; shaking; optical yield given as percent de;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4876 - 4878
反应条件
hydrogen; silica gel; palladium T=-0.15°C; P=150.012 Torr; also ethyloxirane; also with duterium; also over Pt-SiO2; var. temp. and time; Product distributionMechanism;
参考文献
Bartok, Mihaly; Fasi, Andras; Notheisz, Ferenc
Journal of Catalysis, 1998 , vol. 175, # 1 p. 40 - 47
反应条件
water; molybdenum-containing silicate T=25°C; 5 h; Product distribution / selectivity;
参考文献
Bissinger et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 2959
反应条件
in tetrahydrofuran; water
参考文献
Sumitomo Chemical Company, Limited
Patent: EP1801227 A1, 2007 ;
反应条件
sulfuric acid 3 h; Heating;
参考文献
Carpita, Adriano; Rossi, Renzo
Synthesis, 1982 , # 6 p. 469 - 471
反应条件
tert.-butylhydroperoxide; molybdenum resinate in toluene T=110°C;
参考文献
Mel'nik; Nozhnin; Grechina; Kryukov; Yegorova; Danilova
Petroleum Chemistry, 1996 , vol. 36, # 5 p. 455 - 459
反应条件
potassium iodide; USY zeolite in various solvent(s) T=74.85°C; 24 h; var. nucleophiles and acids; var. solv. and time; Product distributionMechanism;
参考文献
Remans, Thomas J.; Van Oeffelen, Domien; Steijns, Matt; Martens, Johan A.; Jacobs, Pierre A.
Journal of Catalysis, 1998 , vol. 175, # 2 art. no. CA982018, p. 312 - 315