1,2-二氢-3H-1,2,4-三氮唑-3-酮合成路线 (共 11 条)
反应条件
trimethyl orthoformate in methanol; toluene
参考文献
Cowden, Cameron John
Patent: US2003/187274 A1, 2003 ;
反应条件
in water T=106°C; 4 h;
参考文献
Fan, Leimin; Dass, Chhabil; Burkey, Theodore J.
Journal of Labelled Compounds and Radiopharmaceuticals, 1996 , vol. 38, # 1 p. 87 - 94
反应条件
T=800°C; P=0.01 Torr;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 50 - 55
参考文献
Haines, David R.; Leonard, Nelson J.; Wiemer, David F.
Journal of Organic Chemistry, 1982 , vol. 47, # 3 p. 474 - 482
反应条件
acetic acid; sodium nitrite Deamination; 4 h;
参考文献
Le Campion; De Suzzoni-Dezard; Robic; Vandais; Varenne; Noel; Ouazzani
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1203 - 1213
反应条件
T=800°C; P=0.01 Torr;
参考文献
Heteroatom Chemistry, , vol. 14, # 1 p. 50 - 55
参考文献
Rozin, Yu. A.; Belyaev; Bakulev; Leban; Azev, Yu. A.
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 12 p. 1534 - 1535
参考文献
Journal of the American Chemical Society, , vol. 79, p. 2839,2843
参考文献
Annali di Chimica (Rome, Italy), , vol. 49, p. 1649,1656, 1663
反应条件
in methanol; diethyl ether T=0°C; Further byproducts given;
参考文献
Bojarska-Olejnik, Elzbieta; Stefaniak, Lech; Witanowski, Michal; Webb, Graham A.
Bulletin of the Polish Academy of Sciences, Chemistry, 1986 , vol. 34, # 7-8 p. 295 - 303