(2,2-二甲基环丙基)甲醇合成路线 （共 15 条）
反应条件
potassium hydroxide; potassium permanganate in water 2 h; Heating;
参考文献
Allen; Fenwick; Henry-Riyad; Tidwell
Journal of Organic Chemistry, 2001 , vol. 66, # 17 p. 5759 - 5765
反应条件
1: diiodomethane With diethylzinc in dichloromethane
T=0°C; 0.25 h;
2: 3,3-dimethylallyl alcohol in dichloromethane
T=-20°C; 0.25 h;
3: With titanium tetrachloride in dichloromethane
T=-20°C; 2 h; Further stages.;
参考文献
Charette; Molinaro; Brochu
Journal of the American Chemical Society, 2001 , vol. 123, # 49 p. 12160 - 12167
反应条件
titanium tetrachloride in dichloromethane
T=-20°C;
参考文献
Charette, Andre B.; Brochu, Christian
Journal of the American Chemical Society, 1995 , vol. 117, # 45 p. 11367 - 11368
反应条件
1: allyl alcohol With diethylzinc in dichloromethane
T=-10°C; 0.166667 h;
2: 2,2-diiodopropane in dichloromethane
T=20°C; 16 h;
参考文献
Charette; Wilb
Synlett, 2002 , # 1 p. 176 - 178
反应条件
lithium aluminium tetrahydride
参考文献
Bly,R.S.; Swindell,R.T.
Journal of Organic Chemistry, 1965 , vol. 30, p. 10 - 22
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Binns,T.D. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2499 - 2501
反应条件
1: 60 percent / LiAlH4 / diethyl ether / 1.5 h / ice bath
2: 36 percent / triethylbenzylammonium chloride, NaOH / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Richey, Herman G.; Moses, L. Meredith
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4013 - 4017
反应条件
1: 36 percent / triethylbenzylammonium chloride, NaOH / H2O / 24 h / Ambient temperature
View Scheme
参考文献
Richey, Herman G.; Moses, L. Meredith
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 4013 - 4017
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Zimmermann,H.E.; Klun,R.T.
Tetrahedron, 1978 , vol. 34, p. 1775 - 1803
反应条件
2: LiAlH4
View Scheme
参考文献
Binns,T.D. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2499 - 2501
反应条件
(i) LiAlH4, Et2O, (ii) H2O; Multistep reaction;
参考文献
Salomon,R.G. et al.
Journal of Organic Chemistry, 1975 , vol. 40, # 6 p. 756 - 760
