反应条件
1: 1) n-BuLi / 1) ether, hexane, -78 deg C, 5 min, 2) a) to 23 deg C, 2 h, b) 23 deg C, 8 h
2: 89 percent / imidazole / tetrahydrofuran / 8 h / 23 °C
3: 74 percent / LiClO4 / diethyl ether / 24 h / 23 °C
4: 97 percent / LiAlH4 / tetrahydrofuran / 1 h / 0 °C
5: Et3N / CH2Cl2 / 1 h / -50 °C
6: Bu4NN3 / tetrahydrofuran / 2 h
7: Bu4NN3 / tetrahydrofuran / 9 h
View Scheme
参考文献
Pearson, William H.; Schkeryantz, Jeffrey M.
Tetrahedron Letters, 1992 , vol. 33, # 37 p. 5291 - 5294
