反应条件
in acetone
byproducts: AgBr; (N2), Schlenk techniques; mixing Au complex, acetone, cooling to -40°C, addn. of mixture of Ag compd., NaSPh (3 equiv.), warming to room temp., stirring for 4 h; filtration (Celite), evapn., dissolving in CH2Cl2 and slow gas diffusionof Et2O or crystn. (CH2Cl2/Et2O), NMR, XRD;
参考文献
Hirtenlehner, Christa; Krims, Charlotte; Hoelbling, Johanna; List, Manuela; Zabel, Manfred; Fleck, Michel; Berger, Raphael J. F.; Schoefberger, Wolfgang; Monkowius, Uwe
Dalton Transactions, 2011 , vol. 40, # 38 p. 9899 - 9910
