in tetrahydrofuran
in foil wrapped tube; Zr complex and MeN(CO)2CHCH (1 equiv.) dissolved in THF; Ph2SbCl3 (1 equiv.) added; stirred for 3 h; crystd. from hexane at 5°C (Ph2SbCl); detd. by single crystal X-ray diffraction;
参考文献
Fish, Cheryl; Green, Michael; Kilby, Richard J.; McGrady, John E.; Pantazis, Dimitrios A.; Russell, Christopher A.
Dalton Transactions, 2008 , # 28 p. 3753 - 3758
Warrener, Ronald N.; Harrison, Peter A.; Sterns, Meta; Russell, Richard A.
Journal of the Chemical Society, Chemical Communications, 1984 , # 8 p. 546 - 548
1: With bromine in diethyl ether
1 h; Reflux;
2: With triethylamine in diethyl ether
T=0 - 18°C;
参考文献
Banwell, Martin G.; Jones, Matthew T.; Loong, David T.J.; Lupton, David W.; Pinkerton, David M.; Ray, Jayanta K.; Willis, Anthony C.
Tetrahedron, 2010 , vol. 66, # 47 p. 9252 - 9262
McKenzie, Thomas C.; Epstein, Joseph W.; Fanshawe, William J.; Dixon, J. Scott; Osterberg, Arnold C.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 5 p. 628 - 632
Epstein, Joseph W.; McKenzie, Thomas C.; Lovell, M. F.; Perkinson, Nancy A.
Journal of the Chemical Society, Chemical Communications, 1980 , # 7 p. 314 - 315
Epstein, Joseph W.; McKenzie, Thomas C.; Lovell, M. F.; Perkinson, Nancy A.
Journal of the Chemical Society, Chemical Communications, 1980 , # 7 p. 314 - 315
