2-(羟基甲基)环戊烯-2-酮合成路线 （共 15 条）
反应条件
4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=0°C; 0.25 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 735 - 737
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1953 , vol. 75, p. 939,940
反应条件
1: TsOH / benzene / 4 h / Heating 2: LiAlH4 View Scheme
参考文献
Bardou,L. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 297 - 306
反应条件
1: cyanoacetic acid amide; piperidine; aqueous ethanol 2: hydrochloric acid; water / 160 °C 3: phosphoryl chloride; phosphorus (V)-chloride / 130 °C View Scheme
参考文献
Thompson
Journal of the American Chemical Society, 1931 , vol. 53, p. 3160,3162
反应条件
1: K2CO3 / acetone 2: diethyl ether; tetrahydrofuran View Scheme
参考文献
Nasipuri,D.; Biswas,K.K.
Journal of the Indian Chemical Society, 1967 , vol. 44, p. 620 - 627
反应条件
1: K2CO3 / acetone 2: diethyl ether; tetrahydrofuran 3: aq. HCl / methanol View Scheme
参考文献
Nasipuri,D.; Biswas,K.K.
Journal of the Indian Chemical Society, 1967 , vol. 44, p. 620 - 627
反应条件
methanol; sodium in diethyl ether
T=20°C; 24 h;
参考文献
Sangeetha; Prasad, K.J. Rajendra
Heterocyclic Communications, 2002 , vol. 8, # 1 p. 65 - 70
反应条件
(i) COCl2, CH2Cl2, (ii) /BRN= 117154/; Multistep reaction;
参考文献
Ziegenbein,W.
Angewandte Chemie, 1965 , vol. 77, p. 380
反应条件
toluene-4-sulfonic acid in benzene
4 h; Heating;
参考文献
Bardou,L. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 297 - 306
反应条件
sulfuric acid; sodium acetate; acetic acid
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1903 , vol. 329, p. 116
