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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
93008-63-0
合成路线
（共 9 条）
371153-68-3
→
反应条件
93008-63-0
反应条件
hydrogen; Pd on fibroin in methanol T=20°C; 12 h;
参考文献
Hattori, Tomohiro; Tsubone, Aya; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2014 , vol. 70, # 32 p. 4790 - 4798
227778-64-5
→
反应条件
93008-63-0
反应条件
4,4'-diphenylsulfide; hydrogen; palladium on activated charcoal in methanol T=20°C; P=760 Torr; 24 h;
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 51 p. 11925 - 11932
371153-68-3
→
反应条件
93008-63-0
+
589-16-2
4-乙基苯胺
反应条件
palladium on activated charcoal; hydrogen in methanol T=20°C; 24 h; chemoselective reaction;
参考文献
Esaki, Hiroyoshi; Hattori, Tomohiro; Tsubone, Aya; Mibayashi, Satoko; Sakata, Takao; Sawama, Yoshinari; Monguchi, Yasunari; Yasuda, Hidehiro; Nosaka, Kazuto; Sajiki, Hironao
ChemCatChem, 2013 , vol. 5, # 12 p. 3629 - 3635
227778-64-5
→
反应条件
93008-63-0
+
589-16-2
4-乙基苯胺
反应条件
hydrogen; palladium on activated charcoal in tetrahydrofuran T=20°C; 1 h;
参考文献
Ikawa, Takashi; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2005 , vol. 61, # 8 p. 2217 - 2231
13139-17-8
苯甲氧羰酰琥珀酰亚胺
→
反应条件
93008-63-0
反应条件
1: 92 percent / tetrahydrofuran / 7 h 2: 98 percent / diphenylsulfide; hydrogen / palladium on activated carbon / methanol / 24 h / 20 °C / 760 Torr View Scheme
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 51 p. 11925 - 11932
1520-21-4
4-乙烯苯胺
→
反应条件
93008-63-0
反应条件
1: 92 percent / tetrahydrofuran / 7 h 2: 98 percent / diphenylsulfide; hydrogen / palladium on activated carbon / methanol / 24 h / 20 °C / 760 Torr View Scheme
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2006 , vol. 62, # 51 p. 11925 - 11932
371153-68-3
→
反应条件
93008-63-0
+
227778-64-5
反应条件
hydrogen in 1,4-dioxane; methanol T=20°C; 24 h; chemoselective reaction;
参考文献
Sajiki, Hironao; Mori, Shigeki; Ohkubo, Tomoyuki; Ikawa, Takashi; Kume, Akira; Maegawa, Tomohiro; Monguchi, Yasunari
Chemistry - A European Journal, 2008 , vol. 14, # 17 p. 5109 - 5111
14235-81-5
4-乙炔基苯胺
→
反应条件
93008-63-0
反应条件
1: 93 percent / tetrahydrofuran / 36 h / 20 °C 2: 92 percent / hydrogen / palladium on silk-fibroine / methanol / 32 h / 20 °C / 2280 Torr View Scheme
参考文献
Ikawa, Takashi; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2005 , vol. 61, # 8 p. 2217 - 2231
501-53-1
氯甲酸苄酯
+
589-16-2
4-乙基苯胺
→
反应条件
93008-63-0
反应条件
triethylamine in dichloromethane 48 h; Heating;
参考文献
Pati, Hari; Weisbruch, Paul; Lemon, Adrienne; Lee, Moses
Synthetic Communications, 2004 , vol. 34, # 5 p. 933 - 940
