(1R,2R)-(-)-2-氨基环己醇合成路线 （共 31 条）
反应条件
sodium hydroxide in ethanol T=20°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 78, # 17 p. 8465 - 8484
参考文献
Bulletin de la Classe des Sciences, Academie Royale de Belgique, , vol. <5> 22, p. 924,926, 931
Bulletin des Societes Chimiques Belges, , vol. 46, p. 13,14, 18
反应条件
1: 16 percent / 0.5 h / 130 °C 2: 36 percent / CH2Cl2 / 1 h / 10 °C / Irradiation 3: KOH / various solvent(s) / 0.08 h / 160 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1553 - 1561
反应条件
1: 36 percent / CH2Cl2 / 1 h / 10 °C / Irradiation 2: KOH / various solvent(s) / 0.08 h / 160 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1553 - 1561
反应条件
1: 0.23 h / 20 °C / |Ionic liquid 2: sodium cyanoborohydride; acetic acid / 36 h / 20 °C 3: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 43, # 4 p. 505 - 519
反应条件
1: sodium cyanoborohydride; acetic acid / 36 h / 20 °C 2: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Synthetic Communications, , vol. 43, # 4 p. 505 - 519
反应条件
1: Raney nickel; ethanol / 180 °C / 73550.8 Torr / Hydrogenation 2: aqueous hydrochloric acid View Scheme
反应条件
1: diethyl ether; silver oxide 2: water; ammonia / 110 - 115 °C View Scheme
参考文献
Annales de Chimie (Cachan, France), , vol. <8> 6, p. 208
Bulletin de la Societe Chimique de France, , vol. <3> 33, p. 269
反应条件
Yield given. Multistep reaction;
参考文献
Polish Journal of Chemistry, , vol. 64, # 7 p. 613 - 618
