反应条件
1: 98 percent / conc. sulfuric acid, conc.nitric acid / 2 h / 160 °C 2: 1.) dimethyl sulfate / 1.) 65-70 deg C, 2 h, 2.) water, overnights 3: 1.) 90percent sulfuric acid 2.) aq. sodium nitrite / 1.) 120 deg C, 2 h, 2.) 20-25 deg C, 1 h, 80 deg C, 1 h View Scheme
参考文献
Hoare, Jason L.; Cavell, Kingsley J.; Hecker, Richard; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 11 p. 2197 - 2205
