反应条件
in neat (no solvent) The mixt. of PdCl2 and cyclooctene were left under a N2 atm. at 45°C for 3 h, the soln. og PhN3 was added and the temp. was raised to 70-75°C, 6.5 h of heating;; cooled overnight, ppt. was filtered off, washed with n-hexane, crystd.from CH2Cl2-n-hexane, dried in vac.; elem. anal.;;
参考文献
Porta, Francesca; Pizzotti, Maddalena; Monica, Gerolamo La; Finessi, Luis A.; Cenini, Sergio; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 2409 - 2414
