4,5-二氯-3-羟基哒嗪合成路线 (共 68 条)
反应条件
triethylamine in dichloromethane T=25°C; 0.0833333 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
triethylamine in dichloromethane T=-10°C; 0.166667 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
triethylamine in dichloromethane T=-10°C; 0.166667 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
triethylamine in dichloromethane T=25°C; 0.0833333 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=20°C; 0.33 h;
参考文献
Kweon, Deok-Heon; Kim, Ho-Kyun; Kim, Jeum-Jong; Chung, Hyun A.; Woo, Song Lee; Kim, Sung-Kyu; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 1 p. 203 - 211
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=20°C; 0.17 h;
参考文献
Kweon, Deok-Heon; Kim, Ho-Kyun; Kim, Jeum-Jong; Chung, Hyun A.; Woo, Song Lee; Kim, Sung-Kyu; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 1 p. 203 - 211
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Kweon, Deok-Heon; Kim, Ho-Kyun; Kim, Jeum-Jong; Chung, Hyun A.; Woo, Song Lee; Kim, Sung-Kyu; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 1 p. 203 - 211
反应条件
trichlorophosphate T=120°C; 24 h;
参考文献
CENTRO NACIONAL DE INVESTIGACIONES ONCOLOGICAS (CNIO); MCNEENEY, Stephen, Phillip; PASTOR FERNÁNDEZ, Joaquín; MARTÍNEZ GONZÁLES, Sonia; MARTÍN HERNANDO, José Ignacio; RODRÍGUEZ HERGUETA, Antonio; RICO FERREIRA, María del Rosario; BLANCO APARICIO, Carmen
Patent: WO2013/4984 A1, 2013 ;
Location in patent: Page/Page column 70 ;
反应条件
potassium carbonate in acetone T=55°C; 8 h;
参考文献
F. HOFFMANN-LA ROCHE AG; JAESCHKE, Georg; LINDEMANN, Lothar; VIEIRA, Eric; WICHMANN, Juergen
Patent: WO2011/6910 A1, 2011 ;
Location in patent: Page/Page column 35; 36 ;
WO 2011/006910 A1
反应条件
potassium carbonate in N,N-dimethyl-formamide T=50 - 60°C; 2 h;
参考文献
Cho, Su-Dong; Choi, Woo-Yong; Yoon, Yong-Jin
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1579 - 1582