1,2-二氢-5-硝基-3H-1,2,4-三唑-3-酮合成路线 (共 5 条)
反应条件
hydrogenchloride Substitution; 7 h; Heating;
参考文献
Le Campion; De Suzzoni-Dezard; Robic; Vandais; Varenne; Noel; Ouazzani
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1203 - 1213
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; Reduction; P=1551.44 Torr; 5 h;
参考文献
Le Campion; De Suzzoni-Dezard; Robic; Vandais; Varenne; Noel; Ouazzani
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 12 p. 1203 - 1213
反应条件
sodium sulfate in water pH=2 - 7; Electrolysis;
参考文献
Wallace, Lynne; Underwood, Christie J.; Day, Anthony I.; Buck, Damian P.
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2894 - 2901
反应条件
1: With sulfuric acid in water T=20°C; Electrolysis; 2: With sodium sulfate; sodium hydroxide in water pH=8; 8 h; Electrolysis; 3: in water T=80°C; 0.0833333 h;
参考文献
Wallace, Lynne; Underwood, Christie J.; Day, Anthony I.; Buck, Damian P.
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2894 - 2901
反应条件
1: With sulfuric acid in water T=20°C; Electrolysis; 2: With sodium sulfate; sodium hydroxide in water pH=8; 8 h; Electrolysis;
参考文献
Wallace, Lynne; Underwood, Christie J.; Day, Anthony I.; Buck, Damian P.
New Journal of Chemistry, 2011 , vol. 35, # 12 p. 2894 - 2901