tetrakis(triphenylphosphine) palladium(0) in toluene T=75°C; 7 h; var. palladium catalysts; other 5-substituted-1-aza-5-stannabicyclo<3.3.3>undecanes and aryl bromides; 1-iodo-heptene; Product distribution;
参考文献
Vedejs, Edwin; Haight, Anthony R.; Moss, William O.
Journal of the American Chemical Society, 1992 , vol. 114, # l6 p. 6556 - 6558
in diethyl ether
byproducts: LiCl; dropping LiCH3 in ether to a suspension of the chloride in ether at -78°C under stirring; filtration;; recrystallization from acetone, elem. anal.;;
参考文献
Jurkschat, K.; Tzschach, A.
Journal of Organometallic Chemistry, 1984 , vol. 272, # 1 p. C13 - C16
