6-溴-1,2-苯并异噻唑-3-羧酸叔丁酯合成路线 (共 2 条)
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran; tert-butyl alcohol
T=65°C; 16 h;
参考文献
MEMORY PHARMACEUTICALS CORPORATION
Patent: WO2007/56582 A1, 2007 ;
Location in patent: Page/Page column 69-70 ;
WO 2007/056582 A1
反应条件
4-(N,N-dimethlyamino)pyridine in tetrahydrofuran
T=65°C; 16 h;
参考文献
Schumacher, Richard; Danca, Mihaela Diana; Ma, Jianguo; Herbert, Brian; Nguyen, True Minh; Xie, Wenge; Tehim, Ashok
Patent: US2007/78147 A1, 2007 ;
Location in patent: Page/Page column 62 ;