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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
93273-60-0
合成路线
（共 6 条）
3360-52-9
+
10365-98-7
3-甲氧基苯硼酸
→
反应条件
93273-60-0
反应条件
palladium (II) trifluoroacetate; potassium hydroxide in water T=90°C; Suzuki Coupling; 3 h; Green chemistry;
参考文献
Dong, Chaonan; Zhang, Lingjuan; Xue, Xiao; Li, Huanrong; Yu, Zhiyong; Tang, Weijun; Xu, Lijin
RSC Advances, 2014 , vol. 4, # 22 p. 11152 - 11158
3360-54-1
(1-溴甲基-乙烯基)-苯
+
10365-98-7
3-甲氧基苯硼酸
→
反应条件
93273-60-0
反应条件
palladium (II) trifluoroacetate; potassium hydroxide in water T=90°C; Suzuki Coupling; 3 h; Green chemistry; Catalytic behavior; Reagent/catalyst;
参考文献
Dong, Chaonan; Zhang, Lingjuan; Xue, Xiao; Li, Huanrong; Yu, Zhiyong; Tang, Weijun; Xu, Lijin
RSC Advances, 2014 , vol. 4, # 22 p. 11152 - 11158
93273-52-0
→
反应条件
93273-60-0
+
93273-59-7
+
93273-53-1
反应条件
in N,N-dimethyl-formamide 12 h; Ambient temperature;
参考文献
Malik, Mangel S.; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 834 - 838
93300-81-3
→
反应条件
93273-60-0
反应条件
1: 95 percent / H2SO4 / 12 h / Heating 2: 66 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature 3: 70 percent / pyridine / 12 h / Ambient temperature 4: dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Malik, Mangel S.; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 834 - 838
93273-51-9
→
反应条件
93273-60-0
反应条件
1: 70 percent / pyridine / 12 h / Ambient temperature 2: dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Malik, Mangel S.; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 834 - 838
93273-50-8
→
反应条件
93273-60-0
反应条件
1: 66 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature 2: 70 percent / pyridine / 12 h / Ambient temperature 3: dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Malik, Mangel S.; Rastogi, Shri Nivas
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 834 - 838
