1: 95 percent / dimethylformamide / 20 °C / electrolysis; anode: platinum, cathode: mercury pool; lithium perchlorate, potential of -1V (vs saturated calomel electrode) 2: 74 percent / aq. 15percent HCl, HgCl2 / 6 h / Heating View Scheme

1: 95 percent / anhydrous lithium perchlorate, anhydrous sodium carbonate, sodium thiosulfate / dimethylformamide / 20 °C / electrolysis 2: 73 percent / dimethylformamide / 1 h / Heating View Scheme

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a> <br />&nbsp;Yield given;&nbsp;<br /> &nbsp;