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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
93321-11-0
合成路线
（共 31 条）
68211-49-4
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
93321-11-0
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
68211-49-4
+
16750-63-3
2-甲氧基苯基溴化镁
→
反应条件
93321-11-0
反应条件
1: 2-methoxy-phenylmagnesium bromide With C24H52Cl2O12P4Pd2 in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada-Corriu cross-coupling reaction; 0.0833333 h; Inert atmosphere; 2: 1−naphthyltosylate in tetrahydrofuran; 1,4-dioxane T=80°C; Kumada-Corriu cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Fenner, Sabine; Kornhaab, Christoph; Schulzke, Carola
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2965 - 2971
408313-37-1
→
反应条件
93321-11-0
反应条件
iodine; magnesium oxide; xylene
参考文献
Stubbs; Tucker
Journal of the Chemical Society, 1954 , p. 227,233
610-96-8
2-氯苯甲酸甲酯
+
6301-54-8
2-萘-1-基丙-2-醇
→
反应条件
93321-11-0
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 4 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
766-51-8
2-氯苯甲醚
+
630-95-5
alpha,alpha-二苯基萘-1-甲醇
→
反应条件
93321-11-0
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 2 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
38262-42-9
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
93321-11-0
反应条件
anhydrous dipotassium phosphate; [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in 1,4-dioxane T=100 - 110°C; Suzuki-Miyaura coupling reaction; Inert atmosphere;
参考文献
Gao, Han; Li, You; Zhou, Yi-Guo; Han, Fu-She; Lin, Ying-Jie
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 309 - 314
116400-74-9
→
反应条件
93321-11-0
反应条件
selenium T=275°C;
参考文献
Baddar; El-Assal
Journal of the Chemical Society, 1951 , p. 1844,1846
529-28-2
2-碘苯甲醚
+
13922-41-3
1-萘硼酸
→
反应条件
93321-11-0
反应条件
tetrakis(triphenylphosphine) palladium(0); Ba(OH)2·8H2O in ethylene glycol dimethyl ether; water T=80°C; 24 h; Inert atmosphere;
参考文献
Yasuda, Makoto; Nakajima, Hideto; Takeda, Ryosuke; Yoshioka, Sachiko; Yamasaki, Satoshi; Chiba, Kouji; Baba, Akio
Chemistry - A European Journal, 2011 , vol. 17, # 14 p. 3856 - 3867
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
93321-11-0
反应条件
1: diethyl ether; benzene / 20 °C 3: palladium/charcoal / 280 - 320 °C View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
529-34-0
1-四氢萘酮
→
反应条件
93321-11-0
反应条件
1: diethyl ether; benzene / 20 °C 3: palladium/charcoal / 280 - 320 °C View Scheme
参考文献
Orchin
Journal of the American Chemical Society, 1948 , vol. 70, p. 495
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