1-溴-4-(甲基亚磺酰)苯合成路线 （共 19 条）
参考文献
Bulletin de la Classe des Sciences, Academie Royale de Belgique, , vol. <5>12, p. 940,941;
Bulletin des Societes Chimiques Belges, , vol. 36, p. 556;
Chem. Zentralbl., , vol. 98, # I p. 1822
反应条件
potassium superoxide; 2-nitro-benzenesulfonyl chloride in acetonitrile T=-30°C; 5.5 h;
参考文献
KIM, Yong Hae; LEE, Hyeon Kyu
Chemistry Letters, 1987 , p. 1499 - 1502
反应条件
1: With bis(acetylacetonate)oxovanadium; (R)-diiodo Shiff base ligand in chloroform T=22°C; 1 h; 2: With dihydrogen peroxide in chloroform T=0°C; 20 h; Title compound not separated from byproducts;
参考文献
Mohammadpoor-Baltork, Iraj; Hill, Mathias; Caggiano, Lorenzo; Jackson, Richard F. W.
Synlett, 2006 , # 20 p. 3540 - 3544
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in 1,4-dioxane T=85°C; 4 h;
参考文献
WO2009/70873 A1, ;
Page/Page column 51 ;
WO 2009/070873 A1
反应条件
niobium pentachloride; zinc in tetrahydrofuran; benzene T=23°C; 3.5 h; Inert atmosphere;
参考文献
Oh, Kyungsoo; Knabe, William Eric
Tetrahedron, 2009 , vol. 65, # 15 p. 2966 - 2974
反应条件
biscyclopentadienyliron(II) in chloroform T=20°C; Reduction; α-trifluoroacetoxylation; 24 h;
参考文献
Kobayashi, Kenji; Kubota, Yasuo; Furukawa, Naomichi
Chemistry Letters, 2000 , # 4 p. 400 - 401
反应条件
MoO2Cl2(OPPh3)2 in acetonitrile T=60°C; 10 h;
参考文献
Marom, Hanit; Antonov, Svetlana; Popowski, Yanay; Gozin, Michael
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5240 - 5246
反应条件
in tetrahydrofuran T=0°C; Grignard reaction; 1.5 h;
参考文献
Capozzi, Maria Annunziata M.; Cardellicchio, Cosimo; Naso, Francesco; Tortorella, Paolo
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2843 - 2846
反应条件
MoO2Cl2(OPPh3)2 in acetonitrile
T=60°C; 10 h;
参考文献
Marom, Hanit; Antonov, Svetlana; Popowski, Yanay; Gozin, Michael
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5240 - 5246
