苄基 2-乙酰氨基-6-O-(2-乙酰氨基-2-脱氧-beta-吡喃葡萄糖基)-2-脱氧-3-O-beta-吡喃岩藻糖基-alpha-吡喃半乳糖苷合成路线 （共 5 条）
反应条件
methanol; Amberlyst A-26 lt;OH(1-)gt; anion exchange resin
5 h; Ambient temperature;
参考文献
Piskorz; Abbas; Matta
Carbohydrate research, 1984 , vol. 131, # 2 p. 257 - 263
反应条件
1: 58 percent / mercuric cyanide / nitromethane; benzene / 40 h / Ambient temperature
2: 64 percent / 60 percent aq. acetic acid / 0.5 h / 98 °C
3: 47 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 70 °C
4: 93 percent / Amberlyst A-26 <OH(1-)> anion exchange resin, methanol / 5 h / Ambient temperature
View Scheme
参考文献
Piskorz; Abbas; Matta
Carbohydrate research, 1984 , vol. 131, # 2 p. 257 - 263
反应条件
1: 58 percent / mercuric cyanide / nitromethane; benzene / 40 h / Ambient temperature
2: 64 percent / 60 percent aq. acetic acid / 0.5 h / 98 °C
3: 47 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 70 °C
4: 93 percent / Amberlyst A-26 <OH(1-)> anion exchange resin, methanol / 5 h / Ambient temperature
View Scheme
参考文献
Piskorz; Abbas; Matta
Carbohydrate research, 1984 , vol. 131, # 2 p. 257 - 263
反应条件
1: 47 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 70 °C
2: 93 percent / Amberlyst A-26 <OH(1-)> anion exchange resin, methanol / 5 h / Ambient temperature
View Scheme
参考文献
Piskorz; Abbas; Matta
Carbohydrate research, 1984 , vol. 131, # 2 p. 257 - 263
反应条件
1: 64 percent / 60 percent aq. acetic acid / 0.5 h / 98 °C
2: 47 percent / p-toluenesulfonic acid / 1,2-dichloro-ethane / 70 °C
3: 93 percent / Amberlyst A-26 <OH(1-)> anion exchange resin, methanol / 5 h / Ambient temperature
View Scheme
参考文献
Piskorz; Abbas; Matta
Carbohydrate research, 1984 , vol. 131, # 2 p. 257 - 263
