3-溴-2,3-二氢-苯并[h]色烯-4-酮合成路线 （共 5 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane
4 h; Heating;
参考文献
Karnik; Malviya; Kulkarni; Jadhav
European Journal of Medicinal Chemistry, 2006 , vol. 41, # 7 p. 891 - 895
Title/Abstract Full Text View citing articles Show Details
Malviya; Kulkarni; Jaimini; Jadhav; Karnik
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 6 p. 1499 - 1503
反应条件
1: 75 percent / polyphosphoric acid / 1.) 1 h 2.) 4h, heating
2: 67 percent / bromine / dioxane / 1.) 0 deg C, 1 h 2.) 50 to 60 deg C, 2 h
View Scheme
参考文献
Sharma, S. D.; Kaur, Sukhjinder
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 518 - 521
反应条件
1: 80 percent / sodium / 2 h / Heating
2: 75 percent / polyphosphoric acid / 1.) 1 h 2.) 4h, heating
3: 67 percent / bromine / dioxane / 1.) 0 deg C, 1 h 2.) 50 to 60 deg C, 2 h
View Scheme
参考文献
Sharma, S. D.; Kaur, Sukhjinder
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 518 - 521
反应条件
1: 54 percent / P2O5, phosphoric acid / 2 h / 100 °C
2: 60 percent / Br2 / diethyl ether
View Scheme
参考文献
Subramanian, L. M.; Misra, G. S.
Synthesis, 1984 , # 12 p. 1063 - 1065
反应条件
in 1,4-dioxane
T=75 - 80°C; 4 h;
参考文献
Karnik; Malviya; Kulkarni; Jadhav
European Journal of Medicinal Chemistry, 2006 , vol. 41, # 7 p. 891 - 895
