tris-(dibenzylideneacetone)dipalladium(0); zinc(II) chloride; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=28°C; Fukuyama Coupling; 12 h; Schlenk techniqueInert atmosphere;

1: diethyl ether 2: K2cr2O7; aqueous H2SO4; benzene View Scheme

1: chloro-trimethyl-silane / tetrahydrofuran / 4 h / 40 °C / |Schlenk technique; |Inert atmosphere 2: tris-(dibenzylideneacetone)dipalladium(0); tri-cyclo-hexyl-phosphine; zinc(II) chloride / tetrahydrofuran / 12 h / 28 °C / |Schlenk technique; |Inert atmosphere View Scheme