反应条件
1: With (2S,3S)-(+)-di-O-(p-toluoyl)-tartaric acid in methanol T=20 - 35°C; 22 - 27 h; Resolution of racemateHeating / reflux; 2: With methanol; water; hydrogen bromide T=0 - 30°C; 3.5 h; Purification / work up;
参考文献
Bolugoddu, Vijaya Bhaskar; Shukla, Sanjay; Jambula, Mukunda Reddy; Sagyam, Rajeshwar Reddy; Pingili, Ramchandra Reddy; Thirunavakarasu, Ananda Babu
Patent: US2006/9640 A1, 2006 ;
Location in patent: Page/Page column 8 ;
