7-溴-9,9-二己基芴-2-硼酸合成路线 （共 3 条）
反应条件
1: With n-butyllithium in hexane
2: in hexane
3: With hydrogenchloride in hexane; water
T=-78°C;
参考文献
Sun, Han-Sheng; Lee, Chia-Hao; Lai, Chia-Sheng; Chen, Hsin-Lung; Tung, Shih-Huang; Chen, Wen-Chang
Soft Matter, 2011 , vol. 7, # 9 p. 4198 - 4206
反应条件
1.1: sodium hydroxide / dimethyl sulfoxide; water / 12 h / 70 °C
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C
2.2: -78 - 20 °C
3.1: hydrogenchloride / water
View Scheme
参考文献
Wang, Feng; Zhu, Cai-Xia
Asian Journal of Chemistry, 2013 , vol. 25, # 10 p. 5700 - 5702
反应条件
1.1: sodium hydroxide / dimethyl sulfoxide; water / 12 h / 70 °C
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C
2.2: -78 - 20 °C
3.1: hydrogenchloride / water
View Scheme
参考文献
Wang, Feng; Zhu, Cai-Xia
Asian Journal of Chemistry, 2013 , vol. 25, # 10 p. 5700 - 5702
