反应条件
1: 77.9 percent / pyridinium chlorochromate / CH2Cl2 / 1 h / Ambient temperature 2: t-butyl-lithium / 1.) THF, -78 deg C 1 h; 2.) THF, -78 deg C 30 min 3: 23.8 percent / toluene-p-sulphonic acid / dioxane; H2O / 0.17 h / 55 °C View Scheme
参考文献
Nemoto, Hideo; Wu, Xiao-Ming; Kurobe, Hiroshi; Minemura, Kayoko; Ihara, Masataka; at. al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1185 - 1190