4,4-二甲氧基-2,5-环己二烯-1-酮合成路线 （共 49 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Russell, Richard A.; Warrener, Ronald N.
Journal of the Chemical Society, Chemical Communications, 1981 , # 3 p. 108 - 110
反应条件
hexafluoroisopropyl alcohol; 2,3,4,5,6-pentafluorobenzoic acid in dichloromethane
T=0°C; 1 h; Enzymatic reaction; Reagent/catalystSolventTemperatureTimeConcentration; regiospecific reaction;
参考文献
Hu, Yinjun; Kamitanaka, Tohru; Mishima, Yusuke; Dohi, Toshifumi; Kita, Yasuyuki
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5530 - 5543
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 0.5 h;
参考文献
Hu, Yinjun; Kamitanaka, Tohru; Mishima, Yusuke; Dohi, Toshifumi; Kita, Yasuyuki
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5530 - 5543
反应条件
hexafluoroisopropyl alcohol; boron trifluoride diethyl etherate in dichloromethane
T=20°C; 1 h;
参考文献
Hu, Yinjun; Kamitanaka, Tohru; Mishima, Yusuke; Dohi, Toshifumi; Kita, Yasuyuki
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5530 - 5543
反应条件
pyridine
T=125°C; 2 h; Microwave irradiationInert atmosphere;
参考文献
Zhang, Jinzhu; Yin, Zhiwei; Leonard, Patrick; Wu, Jing; Sioson, Kate; Liu, Che; Lapo, Robert; Zheng, Shengping
Angewandte Chemie - International Edition, 2013 , vol. 52, # 6 p. 1753 - 1757
Angew. Chem., 2013 , vol. 125, # 6 p. 1797 - 1801,5
反应条件
pyridine
T=125°C; 2 h; Microwave irradiationInert atmosphere;
参考文献
Zhang, Jinzhu; Yin, Zhiwei; Leonard, Patrick; Wu, Jing; Sioson, Kate; Liu, Che; Lapo, Robert; Zheng, Shengping
Angewandte Chemie - International Edition, 2013 , vol. 52, # 6 p. 1753 - 1757
Angew. Chem., 2013 , vol. 125, # 6 p. 1797 - 1801,5
反应条件
pyridine in chloroform
T=90°C; 6 h; Inert atmosphere;
参考文献
Zhang, Jinzhu; Yin, Zhiwei; Leonard, Patrick; Wu, Jing; Sioson, Kate; Liu, Che; Lapo, Robert; Zheng, Shengping
Angewandte Chemie - International Edition, 2013 , vol. 52, # 6 p. 1753 - 1757
Angew. Chem., 2013 , vol. 125, # 6 p. 1797 - 1801,5
反应条件
in water
Irradiation;
参考文献
Margaretha,P.
Helvetica Chimica Acta, 1976 , vol. 59, p. 661 - 664
反应条件
hydrido(triphenylphosphine)copper(I) hexamer in benzene
2 h; Ambient temperaturepH 7 buffer;
参考文献
Koenig, Thomas M.; Daeuble, John F.; Brestensky, Donna M.; Stryker, Jeffrey M.
Tetrahedron Letters, 1990 , vol. 31, # 23 p. 3237 - 3240
