4-乙基-2,6,7-三氧杂-1-磷杂双环[2.2.2]辛烷-1-硫化物合成路线 (共 2 条)
反应条件
sulfur in toluene
Addition; sulfurization; 6 h; Heating;
参考文献
Tkachenko; Trofimova; Fedoseev
Chemistry of Heterocyclic Compounds, 1999 , vol. 35, # 8 p. 973 - 977
反应条件
1: (EtO)3P, Et3N
2: (i) Br2, (ii) octane-1-thiol
View Scheme
参考文献
Wadsworth,W.S.; Emmons,W.D.
Journal of the American Chemical Society, 1962 , vol. 84, p. 610 - 617