N-(2-丙炔基)-甲烷磺酰胺合成路线 (共 3 条)
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide T=0°C; Inert atmosphere;
参考文献
Teller, Henrik; Corbet, Matthieu; Mantilli, Luca; Gopakumar, Gopinadhanpillai; Goddard, Richard; Thiel, Walter; Fuerstner, Alois
Journal of the American Chemical Society, 2012 , vol. 134, # 37 p. 15331 - 15342
反应条件
pyridine
T=0 - 20°C;
参考文献
UCB PHARMA S.A.
Patent: WO2007/141504 A1, 2007 ;
Location in patent: Page/Page column 62 ;
WO 2007/141504 A1
反应条件
in dichloromethane; ethyl acetate
参考文献
Hoffmann-La Roche Inc.
Patent: US6130239 A1, 2000 ;
US 6130239 A