2-(2-呋喃甲酰基)吡啶合成路线 （共 5 条）
反应条件
hydrogenchloride in water
T=60°C; 2 h; Yield given;
参考文献
Siemanowski, Werner; Witzel, Herbert
Liebigs Annalen der Chemie, 1984 , # 10 p. 1731 - 1739
反应条件
1: furan With n-butyllithium in diethyl ether
2 h; Heating;
2: 2-pyridine carbonitrile in diethyl ether
T=-78 - 20°C;
3: With hydrogenchloride in diethyl ether
参考文献
Chubb; Bryce; Tarbit
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 16 p. 1853 - 1854
反应条件
1: 1.) n-C4H9Li / 1.) ether, n-hexane, -70 deg C; 2.) ether, 4h, from -65 deg C to 20 deg C
2: 1 N HCl / H2O / 2 h / 60 °C
View Scheme
参考文献
Siemanowski, Werner; Witzel, Herbert
Liebigs Annalen der Chemie, 1984 , # 10 p. 1731 - 1739
反应条件
1: 1.) n-C4H9Li / 1.) ether, n-hexane, -70 deg C; 2.) ether, 4h, from -65 deg C to 20 deg C
2: 1 N HCl / H2O / 2 h / 60 °C
View Scheme
参考文献
Siemanowski, Werner; Witzel, Herbert
Liebigs Annalen der Chemie, 1984 , # 10 p. 1731 - 1739
反应条件
1: 1.) n-C4H9Li / 1.) ether, 3 h, reflux; 2.) ether, 4 h, from -60 deg C to 10 deg C
2: 1 N HCl / H2O / 2 h / 60 °C
View Scheme
参考文献
Siemanowski, Werner; Witzel, Herbert
Liebigs Annalen der Chemie, 1984 , # 10 p. 1731 - 1739
