2-苯基-1,3-二四氢呋喃合成路线 （共 152 条）
反应条件
diethyl ether; lithium perchlorate
T=28°C; 0.25 h;
参考文献
Saraswathy, V. Geetha; Sankararaman, S.
Journal of Organic Chemistry, 1994 , vol. 59, # 16 p. 4665 - 4670
反应条件
acetyl chloride in methanol
0.5 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286
反应条件
2: 94 percent / Ph3P, imidazole, I2 / tetrahydrofuran / 1 h / 20 °C
3: 89 percent / NaH / benzene; dimethylformamide / 14 h / 50 °C
4: 76 percent / BH3 - dimethyl sulfide / tetrahydrofuran / 9 h / 75 °C
View Scheme
参考文献
Berlage, Ulrich; Schmidt, Jurgen; Peters, Ulrike; Welzel, Peter
Tetrahedron Letters, 1987 , vol. 28, # 27 p. 3091 - 3094
反应条件
fluorine in monofluoro-trichloromethane
T=-78°C; addition of BCl3; Product distribution;
参考文献
Purrington, Suzanne T.; Woodard, Daniel L.
Journal of Organic Chemistry, 1991 , vol. 56, # 1 p. 142 - 145
反应条件
boron trifluoride diethyl etherate in dichloromethane
-78 deg C, 8 h; RT, overnight;
参考文献
Pandey, Bipin; Khire, Uday R.; Ayyangar, Nagaraj R.
Synthetic Communications, 1989 , vol. 19, # 15 p. 2741 - 2748
反应条件
ammonium chloride; β-cyclodextrin; zinc in water
T=50°C; Barbier-type allylation reaction; 8 h;
参考文献
Surendra; Krishnaveni, N. Srilakshmi; Rao, K. Rama
Tetrahedron Letters, 2006 , vol. 47, # 13 p. 2133 - 2136
反应条件
1: 75 percent / ZnI2 / 0.5 h / 25 °C
2: 50 percent / conc. aq. HCl / 1.) reflux, 1 h; 2.) toluene, reflux, 12 h
View Scheme
参考文献
Kirchmeyer, Stephan; Mertens, Alfred; Arvanaghi, Massoud; Olah, George A.
Synthesis, 1983 , # 6 p. 498 - 500
反应条件
in dichloromethane
T=0 - 20°C;
参考文献
Gafarova; Dekhtyar'; Fatykhov; Spirikhin; Vostrikova; Zlotskii; Dokichev
Russian Chemical Bulletin, 2003 , vol. 52, # 4 p. 1003 - 1008
反应条件
triethylaluminum; diethyl aluminium hydride in hexane; kerosene
10 h; Heating;
参考文献
Volkov; Kravets; Zlot-skii; Rakhmankulov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 1 p. 1419 - 1423
反应条件
diethyl aluminium hydride in hexane; kerosene
20 h; Heating;
参考文献
Volkov; Kravets; Zlot-skii; Rakhmankulov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 1 p. 1419 - 1423
