N-(1-环戊烯基)吗啉合成路线 (共 77 条)
反应条件
hydrogenchloride; triethylamine 1.) CHCl3, 0 to 20 deg C, 24 h, 2.) CHCl3/H2O, 60 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Trabelsi; Cambon
Tetrahedron Letters, 1995 , vol. 36, # 18 p. 3145 - 3148
反应条件
sulfur in ethanol 1) 60 deg C, 3-4 h; 2) room temp., 15 h;
参考文献
Peet, Norton P.; Sunder, Shyam; Barbuch, Robert J.; Vinogradoff, Anna P.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 129 - 134
反应条件
sodium tris(acetoxy)borohydride; acetic acid in 1,2-dichloro-ethane 0.333333 h; Ambient temperature;
参考文献
Abdel-Magid, Ahmed F.; Carson, Kenneth G.; Harris, Bruce D.; Maryanoff, Cynthia A.; Shah, Rekha D.
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3849 - 3862
参考文献
Petrolite Corporation
Patent: US4442286 A1, 1984 ;
反应条件
in diethyl ether 4 h; Ambient temperature;
参考文献
Uher, Michal; Foltin, Jozef; Floch, Lubomir
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 11 p. 2696 - 2702
反应条件
(i) ethyl-hexyl-amine, MeCN, (ii) aq. HCl; Multistep reaction;
参考文献
Opitz,G.
Justus Liebigs Annalen der Chemie, 1961 , vol. 650, p. 122 - 132
反应条件
in acetonitrile 21 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2477 - 2489
反应条件
triethylamine in benzene T=20°C; 24 h;
参考文献
Benedetti, Fabio; Fabrissin, Silvio; Fagotto, Roberto; Risaliti, Amerigo
Gazzetta Chimica Italiana, 1990 , vol. 120, # 10 p. 613 - 618
反应条件
benzoyl chloride 1.) CH2CL2, 0 deg C, 30 min, 2.) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Suwinski, Jerzy; Walczak, Krzysztof
Polish Journal of Chemistry, 1984 , vol. 58, # 10-12 p. 1077 - 1083
参考文献
Armarego,W.L.F.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 986 - 990