N-(1-环戊烯基)吗啉合成路线 （共 77 条）
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Birkofer,L. et al.
Chemische Berichte, 1962 , vol. 95, p. 1495 - 1504
参考文献
Takeda,A. et al.
Journal of Organic Chemistry, 1974 , vol. 39, p. 3098 - 3101
参考文献
Sato,T. et al.
Bulletin of the Chemical Society of Japan, 1977 , vol. 50, p. 2714 - 2730
反应条件
1: 89 percent / diethyl ether / 2 h / Ambient temperature 2: 72 percent / 1N aq. HCl / diethyl ether / 4 h / 35 - 40 °C View Scheme
参考文献
Buttke; Niclas
Synthetic Communications, 1994 , vol. 24, # 22 p. 3241 - 3248
反应条件
in toluene 14 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2709 - 2716
反应条件
hydrogenchloride 1.) benzene, 18 h, 23 deg C 2.) benzene, 0 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Corey, E. J.; Kang, Myung-chol; Desai, Manoj C.; Ghosh, Arun K.; Houpis, Ioannis N.
Journal of the American Chemical Society, 1988 , vol. 110, # 2 p. 649 - 651
反应条件
2: HCl / CH2Cl2; diethyl ether
View Scheme
参考文献
Knowles,A.M.; Lawson,A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1240 - 1243
反应条件
in 1,2,3,4-tetrahydro-naphthalene
14 h; Heating;
参考文献
Rossi; Stradi; Visentin
Tetrahedron, 1990 , vol. 46, # 10 p. 3581 - 3592
反应条件
1: 70 percent / Et3N / CHCl3 / 0.5 h
2: 79 percent / H2 / Adams' platinum oxide / ethanol / 0.5 h
3: 79 percent / Heating
View Scheme
参考文献
Zhang, Pang; Li, Lian-chu
Synthetic Communications, 1986 , vol. 16, # 8 p. 957 - 966
反应条件
in dichloromethane
byproducts: 4-[7-phenyl-bicyclo(3.1.0)hex-1-yl]-morpholine; Ar-atmosphere; addn. of 3 equiv. of morpholine derivative to W-complex soln. (room temp., 1 h); evapn., chromy. (SiO2, petroleum ether/CH2Cl2=9:1);
参考文献
Martin-Vaca, Blanca; Rudler, Henri; Audouin, Max; Nicolas, Muriel; Durand-Reville, Thomas; Vissiere, Brice
Journal of Organometallic Chemistry, 1998 , vol. 567, # 1-2 p. 119 - 126
