N-(1-环戊烯基)吗啉合成路线 (共 77 条)
反应条件
hydrogenchloride in chloroform
T=-15°C; 30 h; other enamines, var. aryllead tricarboxylates; Product distributionMechanism;
参考文献
May, George L.; Pinhey, John T.
Australian Journal of Chemistry, 1982 , vol. 35, # 9 p. 1859 - 1871
反应条件
1: Et3N / 0 °C
2: H2
3: 8.7 percent / toluene / 150 - 260 °C / Heating
View Scheme
参考文献
Zhang, Pang; Li, Lian-chu
Synthetic Communications, 1986 , vol. 16, # 8 p. 957 - 966
反应条件
in 1,4-dioxane
16 h; Heating;
参考文献
Kaiser, Stefan; Smidt, Sebastian P.; Pfaltz, Andreas
Angewandte Chemie - International Edition, 2006 , vol. 45, # 31 p. 5194 - 5197
反应条件
(i) Et3N, CHCl3, (ii) aq. HCl; Multistep reaction;
参考文献
White, Robert H.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6605 - 6607
反应条件
in 1,4-dioxane
2 h; Heating; Yields of byproduct given;
参考文献
Nagibina; Sidorova; Klyuev; Charushin; Chupakhin
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 10 p. 1468 - 1475
反应条件
lithium diisopropyl amide
参考文献
Back, Thomas G.; Gladstone, Patricia L.; Parvez, Masood
Journal of Organic Chemistry, 1996 , vol. 61, # 11 p. 3806 - 3814
反应条件
hydrogenchloride in chloroform
1.) reflux, 6 h; 2.) reflux, 6 h;
参考文献
Oppolzer, Wolfgang; Godel, Thierry
Helvetica Chimica Acta, 1984 , vol. 67, p. 1154 - 1167
参考文献
Kober, Reiner; Hammes, Willi; Steglich, Wolfgang
Angewandte Chemie, 1982 , vol. 94, # 3 p. 213 - 214
反应条件
sodium tetrahydroborate
2.) MeCN, reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ghattas, A.-B.A.G.; Jorgensen, K. A.; Lawesson, S.-O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1982 , vol. 36, # 8 p. 505 - 512
参考文献
Gingrich, Henry L.; Roush, David M.; Saun, William A. Van
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4869 - 4873