N-(1-环戊烯基)吗啉合成路线 （共 77 条）
参考文献
Begley, Michael J.; Mellor, Michael; Pattenden, Gerald
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1905 - 1912
反应条件
ammonia in methanol
T=70°C; 3 h;
参考文献
Tohda; Eiraku; Nakagawa; Usami; Ariga; Kawashima; Tani; Watanabe; Mori
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 10 p. 2820 - 2827
反应条件
hydrogenchloride; triethylamine
1.) acetonitrile, 14 h, reflux, 2.) 1 h, room temperature; Yield given. Multistep reaction;
参考文献
Scholz, Dieter
Monatshefte fuer Chemie, 1984 , vol. 115, p. 655 - 658
反应条件
in diethyl ether
Cycloaddition; ring-expansion; Product distribution; Further Variations:Solvents;
参考文献
Miesch, Michel; Wendling, Florence
European Journal of Organic Chemistry, 2000 , # 20 p. 3381 - 3392
反应条件
(i) COCl2, CH2Cl2, (ii) /BRN= 117154/; Multistep reaction;
参考文献
Ziegenbein,W.
Angewandte Chemie, 1965 , vol. 77, p. 380
反应条件
hydrogenchloride; triethylamine
1.) acetonitrile, 14 h, reflux, 2.) 1 h, room temperature; Yield given. Multistep reaction;
参考文献
Scholz, Dieter
Monatshefte fuer Chemie, 1984 , vol. 115, p. 655 - 658
反应条件
1: 83 percent / Cu(OCOCH3)2 / acetonitrile / 2 h / 0 - 20 °C
2: 78 percent / aq. HCl
View Scheme
参考文献
Kirij; Pasenok; Yagupolskii; Tyrra; Naumann
Journal of Fluorine Chemistry, 2000 , vol. 106, # 2 p. 217 - 221
反应条件
hydrogenchloride
1) DMF, 70 deg C, 7 h, irradiated, 2) r.t., 3 h; Yield given. Multistep reaction;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 645 - 648
反应条件
silica gel
silica-gel column chromatography; Multistep reaction;
参考文献
Jaroch, Stefan; Hoelscher, Peter; Rehwinkel, Hartmut; Suelzle, Detlev; Burton, Gerardine; Hillmann, Margrit; McDonald, Fiona M.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 18 p. 2561 - 2564
反应条件
in 1,4-dioxane
15 h; Heating;
参考文献
Altomare, Cosimo; Cellamare, Saverio; Summo, Luciana; Catto, Marco; Carotti, Angelo; Thull, Ulrike; Carrupt, Pierre-Alain; Testa, Bernard; Stoeckli-Evans, Helen
Journal of Medicinal Chemistry, 1998 , vol. 41, # 20 p. 3812 - 3820
