N-(1-环戊烯基)吗啉合成路线 （共 77 条）
反应条件
1: in benzene
20 h; Reflux;
2: With hydrogenchloride; water in benzene
T=20 - 30°C; 2 h;
参考文献
SHENYANG PHARMACEUTICAL UNIVERSITY
Patent: US2011/60054 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
in methanol
Ambient temperatureor with other enamines, regioselectivity of cyclization reaction; Mechanism;
参考文献
Kaupp, Gerd; Pogodda, Uwe; Atfah, Adnan; Meier, Herbert; Vierengel, Anita
Angewandte Chemie, 1992 , vol. 104, # 6 p. 783 - 785
反应条件
1: in benzene
20 h; Reflux;
2: With hydrogenchloride; water in benzene
T=20 - 30°C; 2 h;
参考文献
SHENYANG PHARMACEUTICAL UNIVERSITY
Patent: US2011/60054 A1, 2011 ;
Location in patent: Page/Page column 4 ;
反应条件
hydrogenchloride; triethylamine
1.) CHCl3, room temp., 15 h, 2.) reflux, 5 h; Yield given. Multistep reaction;
参考文献
Kaga, Harumi; Miura, Masakatsu; Orito, Kazuhiko
Synthesis, 1989 , # 11 p. 864 - 866
反应条件
1: NaOMe / (anodic oxidation)
2: aq. HCl / CHCl3
3: aq. HCl / CHCl3
View Scheme
参考文献
Chiba,T. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 3519 - 3523
反应条件
1 h; Ambient temperature;
参考文献
Singh, Harjit; Singh, Paramjit; Mehta, R. K.
Journal of the Indian Chemical Society, 1984 , vol. 61, # 11;12 p. 1048 - 1049
反应条件
hydrogenchloride
1.) CHCl3, -15 deg C, 30 min, 2.) ether; Yield given. Multistep reaction;
参考文献
May, George L.; Pinhey, John T.
Australian Journal of Chemistry, 1982 , vol. 35, # 9 p. 1859 - 1871
反应条件
in acetonitrile
21 h; Heating;
参考文献
Lochead, Alistair W.; Proctor, George R.; Caton, Michael P. L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2477 - 2489
反应条件
toluene-4-sulfonic acid in benzene
Heating;
参考文献
Birkofer,L. et al.
Chemische Berichte, 1962 , vol. 95, p. 1495 - 1504
Full Text Show Details
Katsin,N.; Ikan,R.
Synthetic Communications, 1977 , vol. 7, p. 185 - 188
反应条件
in chloroform
T=0°C; 3 h;
参考文献
Uher, Michal; Foltin, Jozef; Floch, Lubomir
Collection of Czechoslovak Chemical Communications, 1981 , vol. 46, # 11 p. 2696 - 2702
