disodium hydrogenphosphate; sodium amalgam in methanol T=25°C; 48 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '608317', constants.ctx, '0')">3-chloro-benzenecarboperoxoic acid</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0&deg;C;&nbsp;6&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 77 percent / ZnCl₂ / diethyl ether / 2 h / 25 &deg;C<br />2: MCPBA / CH₂Cl₂ / 6 h / 0 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 4 steps<br /> </b>1: 2.) NEt₃ / 1.) CH₂Cl₂, a.) 25 deg C, 4 d, b.) reflux, 1 d, 2.) 25 deg C, 2 d<br />2: 80 percent / 170 &deg;C<br />3: 77 percent / ZnCl₂ / diethyl ether / 2 h / 25 &deg;C<br />4: MCPBA / CH₂Cl₂ / 6 h / 0 &deg;C<br /> <br /> &nbsp;