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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
93627-32-8
合成路线
（共 7 条）
93627-31-7
→
反应条件
93627-32-8
反应条件
hydrogen; palladium on activated charcoal in methanol 0.5 h; Ambient temperature;
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
624-31-7
4-碘甲苯
→
反应条件
93627-32-8
反应条件
1: 15 g / copper powder / 4 h / 190 - 200 °C 2: 0.9 g / conc. H2SO4 chromium trioxide / acetic acid / 4 h / Ambient temperature 3: 0.25 g / anhyd. triethyl phosphite / 8 h / 170 °C 4: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 5: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 6: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
5344-78-5
4-溴-3-硝基苯甲醚
→
反应条件
93627-32-8
反应条件
1: 15 g / copper powder / 4 h / 190 - 200 °C 2: 0.9 g / conc. H2SO4 chromium trioxide / acetic acid / 4 h / Ambient temperature 3: 0.25 g / anhyd. triethyl phosphite / 8 h / 170 °C 4: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 5: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 6: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
93627-30-6
→
反应条件
93627-32-8
反应条件
1: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 2: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
93627-21-5
→
反应条件
93627-32-8
反应条件
1: 0.9 g / conc. H2SO4 chromium trioxide / acetic acid / 4 h / Ambient temperature 2: 0.25 g / anhyd. triethyl phosphite / 8 h / 170 °C 3: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 4: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 5: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
93627-29-3
→
反应条件
93627-32-8
反应条件
1: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 2: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 3: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
93627-22-6
→
反应条件
93627-32-8
反应条件
1: 0.25 g / anhyd. triethyl phosphite / 8 h / 170 °C 2: 0.33 g / HCl(10percent) / methanol / 0.5 h / Heating 3: 85 percent / aq. NaOH (5percent) / 4 h / Ambient temperature 4: 60 percent / H2 / Pd/C (10percent) / methanol / 0.5 h / Ambient temperature View Scheme
参考文献
Bhatia, S. K.; Kapil, R. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 4 p. 296 - 299
