(Z)-4-(4-氯亚苄基)-2-甲基噁唑-5(4h)-酮合成路线 (共 11 条)
反应条件
1: water; acetone / 6 h / |Reflux 2: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Synthetic Communications, , vol. 43, # 21 p. 2892 - 2897
反应条件
1: water; acetone / 6 h / |Reflux 2: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
反应条件
hydrogenchloride; water 3 h; Reflux;
参考文献
Shi, Lei; Wang, Lu; Wang, Zhi; Zhu, Hai-Liang; Song, Qiao
European Journal of Medicinal Chemistry, 2012 , vol. 47, # 1 p. 585 - 593
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 32 - 35
反应条件
hydrogenchloride; water in acetone 3 h; Heating / reflux;
参考文献
Northwest University
Patent: EP2019090 A1, 2009 ;
Location in patent: Page/Page column 8 ;
反应条件
1: With sodium hydroxide T=80°C; 2: With hydrogenchloride 5 h; Heating;
参考文献
Liu, Si-Jie; Cui, Li-Bo; Xu, Hui-Lan; Wang, Tie-Ying; Hu, Chun; Li, Shuo; Lin, Huang-Quan; Wan, David Chicheong
Heterocycles, 2013 , vol. 87, # 12 p. 2607 - 2614
反应条件
1: water; acetone / 6 h / |Reflux 2: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere View Scheme
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897
参考文献
Subhashini, N. J. Prameela; Hanumanthu, P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 32 - 35
反应条件
1: 3M aq. hydrochloric acid / Heating
2: acetyl chloride
View Scheme
参考文献
Dalla, Vincent; Cotelle, Philippe; Catteau, Jean Pierre
Tetrahedron Letters, 1997 , vol. 38, # 9 p. 1577 - 1580
反应条件
1: water; acetone / 6 h / |Reflux
2: [(S)-BINAPRuCl(benzene)]Cl; hydrogen / methanol / 12 h / 20 - 50 °C / 3750.38 Torr / |Autoclave; |Inert atmosphere
View Scheme
参考文献
Arava, Veera Reddy; Amasa, Srinivasulu Reddy; Goud Bhatthula, Bharat Kumar; Kompella, Laxmi Srinivas; Matta, Venkata Prasad; Subha
Synthetic Communications, 2013 , vol. 43, # 21 p. 2892 - 2897