2-(2-甲基-2-丙烯-1-基)萘合成路线 (共 5 条)
反应条件
caesium carbonate; palladium diacetate; tri-cyclo-hexyl-phosphine in toluene
12 h; Heating;
参考文献
Iwasaki, Masayuki; Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2007 , vol. 129, # 14 p. 4463 - 4469
反应条件
caesium carbonate; palladium diacetate; tri-cyclo-hexyl-phosphine in toluene
12 h; Heating;
参考文献
Iwasaki, Masayuki; Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2007 , vol. 129, # 14 p. 4463 - 4469
反应条件
indium(III) chloride; indium; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=100°C; 2 h;
参考文献
Seomoon, Dong; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1165 - 1168
反应条件
indium(III) chloride; indium; lithium chloride; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide
T=100°C; 2 h;
参考文献
Seomoon, Dong; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 1165 - 1168
反应条件
1: With NiBr2(PPh3)2; magnesium bromide in tetrahydrofuran; toluene
T=20 - 60°C; Inert atmosphere;
2: With ammonium chloride in tetrahydrofuran; water; toluene
参考文献
Sumida, Yuto; Yorimitsu, Hideki; Oshima, Koichiro
Organic Letters, 2010 , vol. 12, # 10 p. 2254 - 2257