1-(苯基硫代)丙烷-2-醇合成路线 （共 33 条）
反应条件
sodium hydroxide in ethanol
1.) heating, 30 min, 2.) reflux;
参考文献
Finkielsztein; Alesso; Lantano; Aguirre; Moltrasio Iglesias
Organic Preparations and Procedures International, 1998 , vol. 30, # 1 p. 117 - 120
反应条件
cobalt(II) chloride in acetonitrile
T=25°C;
参考文献
Iqbal, Javed; Pandey, Anu; Shukla, Alka; Srivastava, Rajiv Ranjan; Tripathi, Sanjay
Tetrahedron, 1990 , vol. 46, # 18 p. 6423 - 6432
反应条件
2,4,6-trichloro-1,3,5-triazine
T=20°C; 0.416667 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Kamble, Vinod T.; Sawant, Sanjay S.
Australian Journal of Chemistry, 2008 , vol. 61, # 3 p. 231 - 234
参考文献
Smith, Kline and French Labor.
Patent: US2774770 , 1951 ;
反应条件
boron trifluoride diethyl etherate in chloroform
1) -30 deg C, 3-4 h, 2) rt, overnight;
参考文献
Comel, Alain; Kirsch, Gilbert; Paquer, Daniel
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 70, # 3/4 p. 229 - 234
参考文献
McManus,S.P. et al.
Journal of Organic Chemistry, 1978 , vol. 43, # 4 p. 647 - 649
反应条件
1: Na / ethanol / 2 h
2: NaBH4 / ethanol
View Scheme
参考文献
Singh, Satwinder; Kumar, Subodh; Chimni, Swapandeep Singh
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2457 - 2462
反应条件
tert.-butyl lithium
1.) THF-pentane, -78 deg C, 2 h, 2.) THF-pentane, HMPA;
参考文献
Rawal, Viresh H.; Akiba, Mitsuo; Cava, Michael P.
Synthetic Communications, 1984 , vol. 14, # 12 p. 1129 - 1140
反应条件
1: bromine / diethyl ether; tetrachloromethane / 0.5 h / 0 °C
2: zinc / tetrahydrofuran / |Reflux
3: water / 0.25 h / 20 °C
View Scheme
参考文献
Propersi, Simona; Tidei, Caterina; Bagnoli, Luana; Marini, Francesca; Testaferri, Lorenzo; Santi, Claudio
Journal of Sulfur Chemistry, 2013 , vol. 34, # 6 p. 671 - 676
反应条件
1: zinc / tetrahydrofuran / |Reflux
2: water / 0.25 h / 20 °C
View Scheme
参考文献
Propersi, Simona; Tidei, Caterina; Bagnoli, Luana; Marini, Francesca; Testaferri, Lorenzo; Santi, Claudio
Journal of Sulfur Chemistry, 2013 , vol. 34, # 6 p. 671 - 676
