反应条件
1: 96 percent / diisobutylaluminum hydride / CH2Cl2 / 1 h / -78 °C
2: 94 percent / CBr4, Ph3P / CH2Cl2 / 3 h / -78 - -60 °C
3: 26 percent / KOH / H2O / 0.67 h
4: 70 percent / acetic acid / H2O / 0.17 h / 120 °C
View Scheme
参考文献
Chen, Kau-Ming; Joullie, Madeleine M.
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3795 - 3796
